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Abstarct
We have discovered distinctive red/gray chips
in all the samples we have studied of the dust
produced by the destruction of the World Trade Center.
Examination of four of these samples, collected from separate sites,
is reported in this paper.
These red/gray chips show marked similarities in all four samples.
One sample was collected by a Manhattan resident about ten minutes
after the collapse of the second WTC Tower, two the next day,
and a fourth about a week later.
The properties of these chips were analyzed using optical microscopy,
scanning electron microscopy (SEM), X-ray energy
dispersive spectroscopy (XEDS), and differential scanning calorimetry (DSC).
The red material contains grains approximately 100 nm across
which are largely iron oxide, while aluminum is contained
in tiny plate-like structures.
Separation of components using methyl ethyl ketone demonstrated
that elemental aluminum is present.
The iron oxide and aluminum are intimately mixed in the red material.
When ignited in a DSC device the chips exhibit large
but narrow exotherms occurring at approximately 430 °C,
far below the normal ignition temperature for conventional thermite.
Numerous iron-rich spheres are clearly observed in the residue
following the ignition of these peculiar red/gray chips.
The red portion of these chips is found to be
an unreacted thermitic material and highly energetic.
Keywords:
JScanning electron microscopy,
X-ray energy dispersive spectroscopy,
Differential scanning calorimetry, DSC analysis,
World Trade Center, WTC dust, 9/11, Iron-rich microspheres,
Thermite, Super-thermite, Energetic nanocomposites, Nano-thermite
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